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1 article(s) from Masai, Hiroshi

Synthesis of an organic-soluble π-conjugated [3]rotaxane via rotation of glucopyranose units in permethylated β-cyclodextrin

Jun Terao,
Yohei Konoshima,
Akitoshi Matono,
Hiroshi Masai,
Tetsuaki Fujihara and
Yasushi Tsuji

Beilstein J. Org. Chem. 2014, 10, 2800–2808, doi:10.3762/bjoc.10.297

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Figure 1: Synthesis of [1]rotaxane by self-inclusion of a host–guest-linked molecule: a) short molecular leng...

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Figure 2: Synthesis of an insulated molecule via flipping phenomenon.

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Scheme 1: The synthetic route to the PMβ-CD based linked [3]rotaxane with a 5,15-di([1,1'-biphenyl]-4-yl)porp...

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Figure 3: The aromatic region of the ¹H NMR spectra of 5 at 25 °C: 1) CDCl₃, 2) CD₃OD, and 3) CD₃OD:D₂O 1:1.

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Scheme 2: Selective synthesis of fixed [3]rotaxane by Suzuki cross-coupling reaction.

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Scheme 3: The synthetic routes to precursor of PM β-CD based insulated oligothiophene.

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Scheme 4: Synthesis of dibromohexa(para-phenylene) with two PMCDs 20.

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Scheme 5: Synthesis of pseudo-linked [3]rotaxanes via double self-inclusion through flipping.

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Figure 4: The aromatic region of the ¹H NMR spectra of 5 at 25 °C: 1) CDCl₃, 2) CD₃OD, and CD₃OD/D₂O 1:1.

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Figure 5: The aromatic region of the ¹H NMR spectra of 20 at 25 °C: 1) CDCl₃, 2) CD₃OD, and CD₃OD/D₂O 1:1.

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Scheme 6: Synthesis of fixed [3]rotaxane via complexation with rhodium porphyrin.

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Figure 6: Partial ROESY NMR spectrum of 26 (400 MHz, CDCl₃) showing the NOEs between aromatic protons of the ...

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Letter

Published 28 Nov 2014

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